Halogen / Chlorine Analyzer

The MIPO 5 SERVOCOULOMETER, is an analyzer used to measure total chlorine (and other halogens) by means of coulometric method.

Its measuring capacity extends from traces (<0.5 ppm) to the high concentrations of total chlorine (> 80%). It is also used to measure chlorine On Chlorinated PVC-C. In addition to the accessories for measuring EOX and POX, we offer complete equipment for AOX dosing by agitation and absorption.

Chlorine and AOX analyzer according to the standard ASTM D4929, ASTM D5194, ISO 9562…

This chlorine analyzer has two furnaces, and ensures complete combustion of your samples. The furnace F1 constitutes a real micro reactor, allowing a great flexibility of use. It allows you to program controlled pyrolysis and combustion of your samples through temperature sequences. With this technology, you will no longer generate soot regardless of the nature of the sample and the position of the furnace (vertical or horizontal).

Technical specifications

Principle: Combustion – Coulomety

Detection Limit: < 0.1 ppm to more than 80%
Quantification: < 0.3 ppm to more than 80%

Accuracy / RSD:

At 0.4 ppm: 7.51 %
At 11 ppm: 0.79 %
At 1000 ppm: 0.46 %

Injections:

20 to 80 µl liquids
10 µL LPG
0.5 to 100 mg solids

Supply Gas:

Oxygen: 99.5 % – 3 bar
Argon: 99.5 % – 3 bar

Electric:

110 V / 230 V
60Hz – 50 Hz
1200 W

Température:

Furnaces F2 25 to 1150°C
Furnaces F1 programmable 25 to 1050°C

Applications
Total Chlorine measurement in Petroleum products, Minerals, Used solvents, Fuels, Waters, Cement, Waste, Coals, Plastics, Oils, Chlorinated PVC, Cokes, Tar, Sediments, Plants…

AOX, POX and EOX Measurement

According standards:
ASTM D4929, ASTM D5808, ASTM D5194, ASTM D6721, UOP 779, ISO 9562, NF EN 12260, NF EN 14077

Modes
- Horizontal furnace configuration / compatible with syringe pusher
  All types of samples: Solids, Liquids, Gaseous
- Vertical furnace configuration / compatible with auto injector
  All types of samples: Solids, Liquids, Gaseous
- AOX by Shaker method or Colum method

- Options
  - Liquid Automatic Sampler up to 50 positions
  - Automatic sampler for Gas and/or LPG, with 2 injections loops.
  - Mini automatic injector, for liquid samples from 5 to seven positions.
  - Auto introductor for solids samples with boat support.

Principle	Combustion – Coulomety
Detection Limit Quantification	< 0.1 ppm to more than 80% Quantification < 0.3 ppm to more than 80%.
Accuracy RSD	At 0.4 ppm At 11 ppm At 1000 ppm RSD 7.51 % 0.79 % 0.46 %.
Injections	20 to 80 µl liquids 10 µL LPG 0.5 to 100 mg solids
Supply: gas	Oxygen Argon 99.5 % – 3 bar 99.5 % – 3 bar
Electric	110 V / 230 V 60Hz – 50 Hz 1200 W
Temperature	Furnaces : F2 25 to 1150°C / F1 programmable 25 to1050 °C.

DIMENSIONS	Length	Height	Depth
VERTICAL CONFIGURATION	66cm	65 cm	56 cm
HORIZONTAL CONFIGURATION	113cm	50cm	43cm